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北山羊角化学成分解析
安梅1,宋华玲2,3,张辛未1,张颖2,尚颖丽2,张贤富2,祖恩东3
1.陕西国际商贸学院 珠宝学院,陕西 西安 712046;2.梧州学院 宝石与艺术设计学院,广西 梧州 543003;3.昆明理工大学 材料科学与工程学院,云南 昆明 650093
摘要:
本文以北山羊角为主要研究对象,利用傅里叶变换红外光谱仪、气相色谱仪和全自动氨基酸分析仪检测分析其红外光谱、脂肪酸和氨基酸成分。结果表明:北山羊角红外光谱主要体现角蛋白组分的特征峰,其中1 540 cm-1、1 653 cm-1、3 061 cm-1归属于角蛋白分子中酰胺类成分;1 454 cm-1、2 875 cm-1、2 963 cm-1归属于角蛋白分子中脂类成分;北山羊角共检测出10种脂肪酸组分,主要成分包括棕榈酸、油酸、山俞酸,它们占脂肪酸总量的53.9%;17种氨基酸组分,总量为976.62 mg/g。
关键词:  北山羊角  国家一级保护动物  红外光谱  脂肪酸  氨基酸
DOI:10.14188/j.ajsh.2021.03.014
分类号:O433.4
基金项目:2021年度广西高校中青年教师科研基础能力提升项目(2021KY0677);2019年度教育部人文社会科学研究青年基金项目资助(19YJC760158)
Chemical composition analysis of Capra sibirica horn
AN Mei1, SONG Hualing2,3, ZHANG Xinwei1, ZHANG Ying2, SHANG Yingli2, ZHANG Xianfu2, ZU Endong3
1.School of Jewelry, Shaanxi Institute of International Trade & Commerce, Xi’an 712046, Shaanxi, China;2.Faculty of Gems and Art Design, Wuzhou University, Wuzhou 543003, Guangxi, China;3.Faculty of Material Science and Engineering , Kunming University of Science and Technology, Kunming 650093, Yunnan, China
Abstract:
Fourier transform infrared spectrometer, gas chromatograph and automatic amino acid analyzer were used to analyze the infrared spectrum, fatty acid and amino acid composition of the Capra Siberia horn. The results showed that the infrared spectrum mainly reflected the characteristic peak of the keratin composition, of which 1 540 cm-1, 1 653 cm-1, and 3 061 cm-1 were assigned to the amide components in the keratin molecule, with 1 454 cm-1, 2 875 cm-1, 2 963 cm-1 assigned to the lipid component. Ten kinds of fatty acid components were detected in Capra Siberia horn, including palmitic acid, oleic acid and sorbic acid, which accounted for 53.9% of the total fatty acids. Seventeen amino acids were also characterized with the total amount of 976.62 mg/g.
Key words:  Capra sibirica horn  first class national protected animal  infrared spectrum  fatty acid  amino acid